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Beilstein J. Org. Chem. 2017, 13, 795–799, doi:10.3762/bjoc.13.79
Graphical Abstract
Scheme 1: Retrosynthetic analysis of D-manno-heptulose.
Scheme 2: Initial attempt on the synthesis of the C4 aldehyde from D-lyxose (5).
Scheme 3: Synthesis of differentially protected ketoheptose building block 2.
Scheme 4: Synthesis of D-manno-heptulose (1).